| Complex |
1 |
| Empirical formula |
C12H8N2O4Pb |
| Formula weight |
451.39 |
| Temperature |
293 (2) |
| Crystal system |
Orthorhombic |
| Space group |
P na21 |
| a/Å |
26.264 (5) |
| b/Å |
7.609 (5) |
| c/Å |
5.832 (5) |
| α/º |
90 |
| β/º |
90 |
| γ/º |
90 |
| V/Å3 |
1165.5 (13) |
| Z |
4 |
| Dc/g cm−3 |
2.573 |
| µ (Mo Kα)/mm−1 |
2.876 |
| F (000) |
832 |
| Reflections collected |
9168 |
| Unique reflections |
2822 |
| R (int) |
0.0459 |
| GOF on F2 |
1.008 |
| Final R indices [I>2sigma(I)] |
R1 = 0.0402, wR2 = 0.0814 |
| R indices (all data) |
R1 = 0.0447, wR2 = 0.0826 |